Return to study ST002700 main page
MB Sample ID: SA270103
| Local Sample ID: | ABC-19770 |
| Subject ID: | SU002805 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004376 | AN004377 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Agilent 1290 Infinity | Agilent 1290 Infinity |
| Column | Waters ACQUITY UPLC BEH C18 (50 x 2.1mm,1.7um) | Waters ACQUITY UPLC BEH C18 (50 x 2.1mm,1.7um) |
| MS Type | ESI | ESI |
| MS instrument type | QTOF | QTOF |
| MS instrument name | Agilent 6546 QTOF | Agilent 6546 QTOF |
| Ion Mode | POSITIVE | NEGATIVE |
| Units | normalized peak heights | normalized peak heights |
MS:
| MS ID: | MS004125 |
| Analysis ID: | AN004376 |
| Instrument Name: | Agilent 6546 QTOF |
| Instrument Type: | QTOF |
| MS Type: | ESI |
| MS Comments: | The quadrupole/time-of-flight (QTOF) mass spectrometers are operated with electrospray ionization (ESI) performing full scan in the mass range m/z 65–1700. Agilent 6546 is equipped with a dual JetStream Source. modes producing both unique and complementary spectra. Instrument parameters are as follows (positive mode) Gas Temp 320°C, Gas Flow 8 l/min, Nebulizer 35 psi, Sheath Gas 350°C, Sheath Gas Flow 11, Capillary Voltage 3500 V, Nozzle Voltage 1000V, Fragmentor 175V, Skimmer 65V. Data (both profile and centroid) are collected at a rate of 5 scans per second. In negative ion mode, Gas Temp 360°C, Gas Flow 9 l/min, Fragmentor 120V, with the other parameters identical to positive ion mode. A reference solution generating ions of 121.050 and 922.007 m/z in positive mode and 119.036 and 966.0007 m/z in negative mode, and these are used for continuous mass correction. |
| Ion Mode: | POSITIVE |
| MS ID: | MS004126 |
| Analysis ID: | AN004377 |
| Instrument Name: | Agilent 6546 QTOF |
| Instrument Type: | QTOF |
| MS Type: | ESI |
| MS Comments: | The quadrupole/time-of-flight (QTOF) mass spectrometers are operated with electrospray ionization (ESI) performing full scan in the mass range m/z 65–1700. Agilent 6546 is equipped with a dual JetStream Source. modes producing both unique and complementary spectra. Instrument parameters are as follows (positive mode) Gas Temp 320°C, Gas Flow 8 l/min, Nebulizer 35 psi, Sheath Gas 350°C, Sheath Gas Flow 11, Capillary Voltage 3500 V, Nozzle Voltage 1000V, Fragmentor 175V, Skimmer 65V. Data (both profile and centroid) are collected at a rate of 5 scans per second. In negative ion mode, Gas Temp 360°C, Gas Flow 9 l/min, Fragmentor 120V, with the other parameters identical to positive ion mode. A reference solution generating ions of 121.050 and 922.007 m/z in positive mode and 119.036 and 966.0007 m/z in negative mode, and these are used for continuous mass correction. |
| Ion Mode: | NEGATIVE |
