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MB Sample ID: SA137209
Local Sample ID: | Control2a |
Subject ID: | SU001693 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 55-82 years |
Gender: | Male and female |
Human Race: | unknown |
Human Ethnicity: | unknown |
Human Medications: | Asprin, ACE inhibitor, statins, cilostazol |
Human Smoking Status: | Controls = 4, CLTI Pre-surgery = 7, and CLTI Amputation = 9 |
Select appropriate tab below to view additional metadata details:
NMR:
NMR ID: | NM000188 |
Analysis ID: | AN002651 |
Instrument Name: | Bruker Avance Neo 600 MHz/54mm console |
Instrument Type: | FT-NMR |
NMR Experiment Type: | 1D-1H |
Field Frequency Lock: | Deuterium |
Standard Concentration: | 0.5 mM DSS |
Spectrometer Frequency: | 600.2328273 MHz |
NMR Probe: | 1.7 mm TXI CryoProbe |
NMR Solvent: | Phosphate buffer (pH 7.2) + 2 mM EDTA + 0.5 mM DSS + 0.2% of sodium azide in deuterated environment |
NMR Tube Size: | 1.7 mm O.D. |
Shimming Method: | Topshim |
Pulse Sequence: | noesypr1d |
Water Suppression: | presat |
Pulse Width: | 90-degree |
Receiver Gain: | 101 |
Offset Frequency: | 2827.31 Hz |
Chemical Shift Ref Cpd: | DSS (4,4-dimethyl-4-silapentane-1-sulfonic acid) |
Temperature: | 25 o C |
Number Of Scans: | 128 scans |
Dummy Scans: | 8 |
Acquisition Time: | 4 s |
Relaxation Delay: | 1 s |
Spectral Width: | 7142.9 Hz |
Num Data Points Acquired: | 28571 |
Real Data Points: | 65536 |
Line Broadening: | 0.22 Hz |
Zero Filling: | 65,536 points |
Apodization: | Exponential |
Baseline Correction Method: | Spline |
Chemical Shift Ref Std: | 0 ppm for DSS |