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MB Sample ID: SA137226
Local Sample ID: | CLTI Pre-surgery1B |
Subject ID: | SU001694 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 55-82 years |
Gender: | Male and female |
Human Race: | unknown |
Human Ethnicity: | unknown |
Human Medications: | Asprin, ACE inhibitor, statins, cilostazol |
Human Smoking Status: | Controls = 4, CLTI Pre-surgery = 7, and CLTI Amputation = 9 |
Select appropriate tab below to view additional metadata details:
NMR:
NMR ID: | NM000189 |
Analysis ID: | AN002652 |
Instrument Name: | Bruker Avance 800 MHz with HR-MAS console |
Instrument Type: | FT-NMR |
NMR Experiment Type: | 1D-1H |
Field Frequency Lock: | Deuterium |
Standard Concentration: | None |
Spectrometer Frequency: | 800 MHz |
NMR Probe: | HR-MAS probe |
NMR Solvent: | For HR-MAS experiments, deuterium oxide was used. |
NMR Tube Size: | 3.2 mm inside diameter plastic insert was used for HR-MAS experiments. |
Shimming Method: | Topshim |
Pulse Sequence: | noesypr1d |
Water Suppression: | presat |
Pulse Width: | 90-degree |
Receiver Gain: | 28.5 |
Offset Frequency: | 4.96 Hz |
Chemical Shift Ref Cpd: | None |
Temperature: | 4 oC |
Number Of Scans: | 256 |
Dummy Scans: | 8 |
Acquisition Time: | 2.0447 s |
Relaxation Delay: | 2 s |
Spectral Width: | 8012.8 Hz |
Num Data Points Acquired: | 16384 points |
Real Data Points: | 65536 |
Line Broadening: | 0.5 Hz |
Zero Filling: | 65,536 points |
Apodization: | Exponential |
Baseline Correction Method: | Spline |
Chemical Shift Ref Std: | Alanine doublet at 1.46 ppm |