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MB Sample ID: SA137230
| Local Sample ID: | Control7B |
| Subject ID: | SU001694 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 55-82 years |
| Gender: | Male and female |
| Human Race: | unknown |
| Human Ethnicity: | unknown |
| Human Medications: | Asprin, ACE inhibitor, statins, cilostazol |
| Human Smoking Status: | Controls = 4, CLTI Pre-surgery = 7, and CLTI Amputation = 9 |
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NMR:
| NMR ID: | NM000189 |
| Analysis ID: | AN002652 |
| Instrument Name: | Bruker Avance 800 MHz with HR-MAS console |
| Instrument Type: | FT-NMR |
| NMR Experiment Type: | 1D-1H |
| Field Frequency Lock: | Deuterium |
| Standard Concentration: | None |
| Spectrometer Frequency: | 800 MHz |
| NMR Probe: | HR-MAS probe |
| NMR Solvent: | For HR-MAS experiments, deuterium oxide was used. |
| NMR Tube Size: | 3.2 mm inside diameter plastic insert was used for HR-MAS experiments. |
| Shimming Method: | Topshim |
| Pulse Sequence: | noesypr1d |
| Water Suppression: | presat |
| Pulse Width: | 90-degree |
| Receiver Gain: | 28.5 |
| Offset Frequency: | 4.96 Hz |
| Chemical Shift Ref Cpd: | None |
| Temperature: | 4 oC |
| Number Of Scans: | 256 |
| Dummy Scans: | 8 |
| Acquisition Time: | 2.0447 s |
| Relaxation Delay: | 2 s |
| Spectral Width: | 8012.8 Hz |
| Num Data Points Acquired: | 16384 points |
| Real Data Points: | 65536 |
| Line Broadening: | 0.5 Hz |
| Zero Filling: | 65,536 points |
| Apodization: | Exponential |
| Baseline Correction Method: | Spline |
| Chemical Shift Ref Std: | Alanine doublet at 1.46 ppm |
