Metabolomics Workbench : NIH Data Repository

MB Sample ID: SA026042

Local Sample ID:	-8_27
Subject ID:	SU000524
Subject Type:	Humans
Subject Species:	Homo sapiens
Taxonomy ID:	9606
Species Group:	Human

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NMR

Sample Preparation:

Sampleprep ID:	SP000531
Sampleprep Summary:	Prior to the NMR measurements, 260 μL of EDTA plasma and 260 μL of a sodium phosphate buffer (75 mmol/L Na2HPO4 in 80%/20% H2O/D2O, pH 7.4; including also 0.08% sodium 3-(trimethylsilyl)propionate-2,2,3,3-d4 and 0.04% sodium azide) was mixed and moved to the NMR tubes. All the liquid handling steps for plasma samples were done with a PerkinElmer JANUS Automated Workstation. The NMR metabolomics laboratory setup combined Bruker AVANCE III 500 MHz and Bruker AVANCE III HD 600 MHz spectrometers

Sampleprep ID:

SP000531

Sampleprep Summary:

Prior to the NMR measurements, 260 μL of EDTA plasma and 260 μL of a sodium phosphate buffer (75 mmol/L Na2HPO4 in 80%/20% H2O/D2O, pH 7.4; including also 0.08% sodium 3-(trimethylsilyl)propionate-2,2,3,3-d4 and 0.04% sodium azide) was mixed and moved to the NMR tubes. All the liquid handling steps for plasma samples were done with a PerkinElmer JANUS Automated Workstation. The NMR metabolomics laboratory setup combined Bruker AVANCE III 500 MHz and Bruker AVANCE III HD 600 MHz spectrometers