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MB Sample ID: SA031891
Local Sample ID: | 8-0A |
Subject ID: | SU000612 |
Subject Type: | Human |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Age Or Age Range: | 60 |
Gender: | male |
Human Race: | Caucasian |
Species Group: | Human |
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Sample Preparation:
Sampleprep ID: | SP000619 |
Sampleprep Summary: | Protein precipitation and drying followed by derivatization via methoxyamine and MSTFA |
Extraction Method: | Protein precipitation |
Sample Derivatization: | 18 mg/mL methoxyamine hydrochloride in pyridine for 30 min at 50°C, followed by trimethylsilylation with N-methyl-N- (trimethylsilyl)trifluoroacetamide (MSTFA) for 30 min at 50°C |
Sample Spiking: | retention-time-lock internal standard of perdeuterated myristic acid |