Summary of Study ST000718

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000515. The data can be accessed directly via it's Project DOI: 10.21228/M83D4G This work is supported by NIH grant, U2C- DK119886.

See: https://www.metabolomicsworkbench.org/about/howtocite.php

This study contains a large results data set and is not available in the mwTab file. It is only available for download via FTP as data file(s) here.

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Study IDST000718
Study TitleTargeted Metabolomics in Pediatric US Population Exposed to Low-Level Heavy Metals
Study TypeMS analysis
Study Summarytargeted assays for 200 SLS kids. TCA-Plus and D4 Steroids (Corticosterone, Cortisol, Cortisone, 11-deoxycortisol, 11-deoxycorticostersone, 18-Hydroxycortisol, 21-Deoxycortisol)
Institute
University of Michigan
DepartmentBiomedical Research Core Facilities
LaboratoryMetabolomics core
Last NameKachman
First NameMaureen
Address6300 Brehm Tower, 1000 Wall Street, Ann Arbor, MI 48105-5714
Emailmkachman@med.umich.edu
Phone(734) 232-8175
Submit Date2017-06-19
Num Groups4
Total Subjects200
Raw Data AvailableYes
Raw Data File Type(s)d
Analysis Type DetailGC-MS/LC-MS
Release Date2018-02-07
Release Version1
Maureen Kachman Maureen Kachman
https://dx.doi.org/10.21228/M83D4G
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

Select appropriate tab below to view additional metadata details:

Project:

Project ID:PR000515
Project DOI:doi: 10.21228/M83D4G
Project Title:Syracuse Lead Study (SRS)
Project Type:MS analysis
Project Summary:Environmental Toxicants, Race, and Cardiovascular Disease Risk in Children
Institute:State University of New York
Department:Chemistry
Laboratory:Bendinskas Lab
Last Name:Bendinskas
First Name:Kestutis
Address:Oswego, New York
Email:kestutis.bendinskas@oswego.edu
Phone:315-312-2696

Subject:

Subject ID:SU000741
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Species Group:Human

Factors:

Subject type: Human; Subject species: Homo sapiens (Factor headings shown in green)

mb_sample_id local_sample_id Race Sex
SA040165S00023832African Female
SA040166S00023829African Female
SA040167S00023888African Female
SA040168S00023974African Female
SA040169S00023947African Female
SA040170S00023978African Female
SA040171S00023837African Female
SA040172S00023865African Female
SA040173S00023823African Female
SA040174S00023930African Female
SA040175S00023980African Female
SA040176S00023931African Female
SA040177S00023932African Female
SA040178S00023881African Female
SA040179S00023879African Female
SA040180S00023950African Female
SA040181S00023857African Female
SA040182S00023954African Female
SA040183S00023862African Female
SA040184S00023956African Female
SA040185S00023871African Female
SA040186S00023961African Female
SA040187S00023964African Female
SA040188S00023878African Female
SA040189S00023949African Female
SA040190S00023962African Female
SA040191S00023873African Female
SA040192S00023821African Female
SA040193S00023934African Female
SA040194S00023915African Female
SA040195S00023985African Female
SA040196S00023810African Female
SA040197S00023795African Female
SA040198S00023808African Female
SA040199S00023989African Female
SA040200S00023987African Female
SA040201S00023988African Female
SA040202S00023800African Female
SA040203S00023811African Female
SA040204S00023917African Female
SA040205S00023927African Female
SA040206S00023816African Female
SA040207S00023918African Female
SA040208S00023981African Female
SA040209S00023906African Female
SA040210S00023814African Female
SA040211S00023990African Female
SA040212S00023907African Female
SA040213S00023913African Male
SA040214S00023955African Male
SA040215S00023867African Male
SA040216S00023874African Male
SA040217S00023912African Male
SA040218S00023872African Male
SA040219S00023916African Male
SA040220S00023870African Male
SA040221S00023883African Male
SA040222S00023943African Male
SA040223S00023889African Male
SA040224S00023887African Male
SA040225S00023895African Male
SA040226S00023936African Male
SA040227S00023928African Male
SA040228S00023903African Male
SA040229S00023944African Male
SA040230S00023946African Male
SA040231S00023880African Male
SA040232S00023910African Male
SA040233S00023924African Male
SA040234S00023925African Male
SA040235S00023884African Male
SA040236S00023929African Male
SA040237S00023877African Male
SA040238S00023960African Male
SA040239S00023864African Male
SA040240S00023805African Male
SA040241S00023831African Male
SA040242S00023830African Male
SA040243S00023803African Male
SA040244S00023977African Male
SA040245S00023836African Male
SA040246S00023835African Male
SA040247S00023834African Male
SA040248S00023806African Male
SA040249S00023826African Male
SA040250S00023815African Male
SA040251S00023986African Male
SA040252S00023984African Male
SA040253S00023817African Male
SA040254S00023818African Male
SA040255S00023825African Male
SA040256S00023822African Male
SA040257S00023820African Male
SA040258S00023812African Male
SA040259S00023838African Male
SA040260S00023853African Male
SA040261S00023852African Male
SA040262S00023963African Male
SA040263S00023920African Male
SA040264S00023959African Male
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Collection:

Collection ID:CO000735
Collection Summary:-
Sample Type:Cultured cells

Treatment:

Treatment ID:TR000755
Treatment Summary:-

Sample Preparation:

Sampleprep ID:SP000748
Sampleprep Summary:-
Sampleprep Protocol Filename:A005 - Amino Acids.pdf

Combined analysis:

Analysis ID AN001122 AN001123 AN001124
Analysis type MS MS MS
Chromatography type GC HILIC HILIC
Chromatography system Agilent 7890N Agilent Agilent
Column Phenomenex Zebron ZB-AAA Amino Acid Analysis 10m x 0.25mm Phenomenex Luna NH2 (150 x 1mm,3um) Phenomenex Luna NH2 (150 x 1mm,3um)
MS Type EI ESI ESI
MS instrument type Single quadrupole QTOF Triple quadrupole
MS instrument name Agilent 5975 Agilent 6520B QTOF Agilent 6490A QQQ
Ion Mode POSITIVE NEGATIVE NEGATIVE
Units uM counts pg/ml

Chromatography:

Chromatography ID:CH000788
Instrument Name:Agilent 7890N
Column Name:Phenomenex Zebron ZB-AAA Amino Acid Analysis 10m x 0.25mm
Chromatography Type:GC
  
Chromatography ID:CH000789
Instrument Name:Agilent
Column Name:Phenomenex Luna NH2 (150 x 1mm,3um)
Flow Rate:0.075 mL/min
Solvent A:100% water; 5 mM ammonium acetate, pH 9.9
Solvent B:100% acetonitrile
Chromatography Type:HILIC
  
Chromatography ID:CH000790
Instrument Name:Agilent
Column Name:Phenomenex Luna NH2 (150 x 1mm,3um)
Chromatography Type:HILIC

MS:

MS ID:MS001017
Analysis ID:AN001122
Instrument Name:Agilent 5975
Instrument Type:Single quadrupole
MS Type:EI
Ion Mode:POSITIVE
Analysis Protocol File:A005_Amino_Acids.pdf
  
MS ID:MS001018
Analysis ID:AN001123
Instrument Name:Agilent 6520B QTOF
Instrument Type:QTOF
MS Type:ESI
Ion Mode:NEGATIVE
Analysis Protocol File:A011_-_Glycolysis-TCA-nucleotides.pdf
  
MS ID:MS001019
Analysis ID:AN001124
Instrument Name:Agilent 6490A QQQ
Instrument Type:Triple quadrupole
MS Type:ESI
Ion Mode:NEGATIVE
Analysis Protocol File:Steroids-D5 analysis.pdf
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