| Metadata details for analysis AN000664 | |
|---|---|
| Study ID | ST000421 |
| Analysis ID | AN000664 |
| Study Title | Type 1 Diabetes poor glycemic control versus control samples |
| Institute | Mayo Clinic |
| Species | Homo sapiens |
| Ion_mode | NEGATIVE |
| MS type | ESI |
| MS Instrument Name | Agilent 6220 TOF |
| MS Instrument Type | TOF |
| Chromatography Instrument Name | Agilent 6220 |
| Chromatography Type | HILIC |
| Chromatography Column | None |
| Solvent A | 1% acetonitrile/99% water; 0.1% formic acid; 5 mM ammonium acetate |
| Solvent B | 95% acetonitrile/5% water; 0.1% formic acid |
| Gradient | 0 min, 0% B; 1 min, 0% B; 3 min, 5% B; 13.0 min, 100% B; 16 min, 100% B; 16.5 min, 0% B; and 20 min, 0% B. |
| Flow rate | 400 µL/min |
| Column Temperature | 50 |
| Retention time units | Minutes |
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