| Metadata details for analysis AN001766 | |
|---|---|
| Study ID | ST001082 |
| Analysis ID | AN001766 |
| Study Title | Combined NMR and MS Analysis of PC patien serum (part-II) |
| Institute | Georgia Institute of Technology |
| Species | Homo sapiens |
| Ion_mode | POSITIVE |
| MS type | ESI |
| MS Instrument Name | Thermo Q Exactive HF hybrid Orbitrap |
| MS Instrument Type | Orbitrap |
| Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
| Chromatography Type | HILIC |
| Chromatography Column | Waters Xbridge BEH HILIC (75 x 2.1mm,2.5um) |
| Solvent A | 5% acetonitrile/95% water; 10 mM ammonium formate; 0.05% ammonium hydroxide |
| Solvent B | 100% acetonitrile; 0.05% ammonium hydroxide |
| Gradient | 0-7.0 min. 63% A; 7.0-7.2 min 5% A with an increased flow rate of 500 µL min-1; 7.2-9.9 min 5% A with a decreased flow rate of 300 µL min-1; and 9.9-10.0 min held at 5% A |
| Flow rate | 300 µL min-1 |
| Column Temperature | 50 |
| Retention time units | Minutes |
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