| Metadata details for analysis AN004215 | |
|---|---|
| Study ID | ST002558 |
| Analysis ID | AN004215 |
| Study Title | Extraction and Untargeted Analysis of Metabolome from Undemineralised Cortical Bone Matrix for Forensic Application |
| Institute | University of Central Lancashire |
| Species | Homo sapiens |
| Ion_mode | NEGATIVE |
| MS type | ESI |
| MS Instrument Name | ABI Sciex 6600 TripleTOF |
| MS Instrument Type | QTOF |
| Chromatography Instrument Name | Thermo Dionex Ultimate 3000 |
| Chromatography Type | HILIC |
| Chromatography Column | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
| Solvent A | 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid |
| Solvent B | 85:15 acetonitrile / 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid in water |
| Gradient | 0 min 96% B 2 min 96% B 22 min 65% B 24 min 65% B 24 min 96% B |
| Flow rate | 0.25 ml/min |
| Column Temperature | 50 °C |
| Retention time units | Minutes |
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