Metadata details for analysis AN005301
Study IDST003237
Analysis IDAN005301
Study TitlePlasma metabolomics of patients diagnosed with Alzheimer's Disease under Acetylcholinesterase Inhibitors treatment
InstituteUniversity of Campinas
SpeciesHomo sapiens
Ion_modePOSITIVE
MS typeESI
MS Instrument NameThermo Q Exactive Orbitrap
MS Instrument TypeOrbitrap
Chromatography Instrument NameThermo Dionex Ultimate 3000
Chromatography TypeReversed phase
Chromatography ColumnSupelco Titan C18 (1.9 μm, 2.1 x 100 mm)
Solvent A40% acetonitrile/60% water; 10 mM ammonium acetate
Solvent B10% acetonitrile/90% isopropanol;10 mM ammonium acetate
GradientThe elution gradient started with 40% B from minutes 0-2, 50% B from minutes 3-6, 70% Bfrom minutes 6.1-8, 100% B from minutes 9-11, and from minutes 12-14 the column was stabilized forthe following run
Flow rate0.250 mL/min
Column Temperature45
Retention time unitsMinutes
Study IDST003237
Analysis IDAN005301
Study TitlePlasma metabolomics of patients diagnosed with Alzheimer's Disease under Acetylcholinesterase Inhibitors treatment
InstituteUniversity of Campinas
SpeciesHomo sapiens
Ion_modePOSITIVE
MS typeESI
MS Instrument NameThermo Q Exactive Orbitrap
MS Instrument TypeOrbitrap
Chromatography Instrument NameThermo Dionex Ultimate 3000
Chromatography TypeReversed phase
Chromatography ColumnSupelco Titan C18 (1.9 μm, 2.1 x 100 mm)
Solvent A40% acetonitrile/60% water; 10 mM ammonium acetate
Solvent B10% acetonitrile/90% isopropanol;10 mM ammonium acetate
GradientThe elution gradient started with 40% B from minutes 0-2, 50% B from minutes 3-6, 70% Bfrom minutes 6.1-8, 100% B from minutes 9-11, and from minutes 12-14 the column was stabilized forthe following run
Flow rate0.250 mL/min
Column Temperature45
Retention time unitsMinutes
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