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MB Sample ID: SA011478
| Local Sample ID: | 9 |
| Subject ID: | SU000270 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Subject:
| Subject ID: | SU000270 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Factors:
| Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
|---|---|---|---|---|
| 9 | SA011478 | FL002865 | positive | HIV status |
| 9 | SA011478 | FL002865 | Yes | Obesity |
| 9 | SA011478 | FL002865 | M | Sex |
| 9 | SA011478 | FL002865 | W | Race |
Collection:
| Collection ID: | CO000261 |
| Collection Summary: | - |
| Collection Protocol Filename: | Koethe_SECIM_collection.txt |
| Sample Type: | Blood |
Treatment:
| Treatment ID: | TR000281 |
| Treatment Protocol Filename: | Koethe_SECIM_treatments.txt |
Sample Preparation:
| Sampleprep ID: | SP000275 |
| Sampleprep Summary: | Amino acid|Organic acid|Acylcarnitines |
| Sampleprep Protocol Filename: | SB_AA_Assay.pdf SB_OA_Assay.pdf SB_Acylcarnitine_Assay.pdf |
Combined analysis:
| Analysis ID | AN000394 | AN000395 | AN000396 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | Reversed phase | Reversed phase | Reversed phase |
| Chromatography system | Agilent 1290 Infinity | Thermo Dionex Ultimate 3000 | Agilent 1290 Infinity |
| Column | Waters AccQ Tag (100 x 2mm,1.7um) | Waters Acquity BEH C18 (100 x 2mm,1.7um) | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| MS Type | ESI | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole | Triple quadrupole |
| MS instrument name | Agilent 6490 QQQ | Thermo Quantiva QQQ | Agilent 6490 QQQ |
| Ion Mode | POSITIVE | POSITIVE | POSITIVE |
| Units | uM | uM |
Chromatography:
| Chromatography ID: | CH001335 |
| Methods Filename: | SB_AA_Assay.pdf |
| Instrument Name: | Agilent 1290 Infinity |
| Column Name: | Waters AccQ Tag (100 x 2mm,1.7um) |
| Column Temperature: | 55 |
| Flow Rate: | 0.7 mL/min |
| Solvent A: | AccQ·Tag Eluent A |
| Solvent B: | accQ·Tag Eluent B |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH001336 |
| Methods Filename: | SB_OA_Assay.pdf |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| Column Temperature: | 45 |
| Flow Rate: | 0.3 mL/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 100% acetonitrile; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH001337 |
| Methods Filename: | SB_Acylcarnitine_Assay.pdf |
| Instrument Name: | Agilent 1290 Infinity |
| Column Name: | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| Chromatography Type: | Reversed phase |
MS:
| MS ID: | MS000338 |
| Analysis ID: | AN000394 |
| Instrument Name: | Agilent 6490 QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | POSITIVE |
| Ion Mode: | POSITIVE |
| MS ID: | MS000339 |
| Analysis ID: | AN000395 |
| Instrument Name: | Thermo Quantiva QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | POSITIVE |
| Ion Mode: | POSITIVE |
| MS ID: | MS000340 |
| Analysis ID: | AN000396 |
| Instrument Name: | Agilent 6490 QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | POSITIVE |
| Ion Mode: | POSITIVE |
