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MB Sample ID: SA011682

Local Sample ID:Urine15
Subject ID:SU000276
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Age Or Age Range:Mean (+SD): 54+8 years
Weight Or Weight Range:Mean (+SD): 76+11 kg; BMI < 30
Gender:males and females (see study design)
Human Race:Caucasian (C) and African American (AA)
Human Medications:None
Human Prescription Otc:None
Human Smoking Status:Non-smokers
Human Alcohol Drug Use:None
Human Inclusion Criteria:Healthy, non-smoking, medication free adults
Species Group:Human

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Subject:

Subject ID:SU000276
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Age Or Age Range:Mean (+SD): 54+8 years
Weight Or Weight Range:Mean (+SD): 76+11 kg; BMI < 30
Gender:males and females (see study design)
Human Race:Caucasian (C) and African American (AA)
Human Medications:None
Human Prescription Otc:None
Human Smoking Status:Non-smokers
Human Alcohol Drug Use:None
Human Inclusion Criteria:Healthy, non-smoking, medication free adults
Species Group:Human

Factors:

Local Sample IDMB Sample IDFactor Level IDLevel ValueFactor Name
Urine15SA011682FL002912MGender
Urine15SA011682FL002912CRace

Collection:

Collection ID:CO000268
Collection Summary:-
Collection Protocol ID:Clean catch urine collection
Collection Protocol Filename:SOP_for_urine_sample_collection
Sample Type:Urine
Collection Method:clean catch into NaN3 coated collection cups
Collection Location:Michigan Clinical Research Unit
Collection Frequency:1
Collection Time:Fasting, between 0830-0930
Volumeoramount Collected:30-50ml
Storage Conditions:Initial 4C then -80C following processing
Collection Vials:Urine collection cup
Collection Tube Temp:RT
Additives:NaN3

Treatment:

Treatment ID:TR000288
Treatment Summary:No treatment

Sample Preparation:

Sampleprep ID:SP000282
Sampleprep Summary:-
Sampleprep Protocol Filename:SOP_for_urine_sample_processing
Processing Method:Centrifugation
Processing Storage Conditions:4C
Extraction Method:N/A
Extract Concentration Dilution:N/A
Extract Enrichment:N/A
Extract Cleanup:N/A
Extract Storage:N/A
Sample Resuspension:N/A

Analysis:

MB Sample ID:SA011682
Analysis ID:AN000405
Laboratory Name:University of Alberta National High Field Nuclear Magnetic Resonance Centre
Analysis Type:NMR
Software Version:VNMRJ 2.2c
Operator Name:Ryan McKay
Chromatography ID:CH000286
Num Factors:3
Num Metabolites:59
  
MB Sample ID:SA011682
Analysis ID:AN000404
Laboratory Name:University of Michigan Biochemical NMR Core Laboratory
Analysis Type:NMR
Software Version:VNMRJ 3.2
Operator Name:Michael Finkel
Chromatography ID:CH000286
Num Factors:3
Num Metabolites:59

NMR:

NMR ID:NM000056
Analysis ID:AN000404
Instrument Name:Agilent 500/54 VNMRS
Instrument Type:FT-NMR
NMR Experiment Type:1D 1H
Shimming Method:Healthy urine quantified metabolite data
Receiver Gain:10% (~0.5mM)
Offset Frequency:500 MHz
Presaturation Power Level:ONE-Probe
Chemical Shift Ref Cpd:D2O
Temperature:5mm
Number Of Scans:Auto shim (gradient shimming), and manual when necessary.
Dummy Scans:1D-NOESY
Acquisition Time:saturation at 80 Hz induced field strength
Relaxation Delay:5.5ms
Real Data Points:around -178Hz
Zero Filling:DSS-d6
Apodization:25C
  
NMR ID:NM000057
Analysis ID:AN000405
Instrument Name:Oxford 600
Instrument Type:FT-NMR
NMR Experiment Type:1D 1H
Shimming Method:Healthy urine quantified metabolite data
Receiver Gain:10% (~0.5mM)
Offset Frequency:600 MHz
Presaturation Power Level:HX probe with Z-axis gradient coils
Chemical Shift Ref Cpd:D2O
Temperature:5mm
Number Of Scans:Auto shim (gradient shimming), and manual when necessary.
Dummy Scans:1D-NOESY
Acquisition Time:saturation at 80 Hz induced field strength
Relaxation Delay:5.5ms
Real Data Points:around -178Hz
Zero Filling:DSS-d6
Apodization:25C
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