Return to study ST000293 main page
MB Sample ID: SA013362
| Local Sample ID: | 196356 |
| Subject ID: | SU000313 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Subject Comments: | Gregory_SECIM_Subjects_20150313.txt |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Subject:
| Subject ID: | SU000313 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Subject Comments: | Gregory_SECIM_Subjects_20150313.txt |
| Species Group: | Human |
Factors:
| Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
|---|---|---|---|---|
| 196356 | SA013362 | FL003136 | Medium | B6 Status |
| 196356 | SA013362 | FL003136 | None | B6 Supplementation |
Collection:
| Collection ID: | CO000307 |
| Collection Summary: | n/a |
| Collection Protocol Filename: | Gregory_SECIM_Collections_20150313.txt |
Treatment:
| Treatment ID: | TR000327 |
| Treatment Summary: | n/a |
| Treatment Protocol Filename: | Gregory_SECIM_Treatment_20150313.txt |
Sample Preparation:
| Sampleprep ID: | SP000321 |
| Sampleprep Summary: | - |
| Sampleprep Protocol Filename: | SB_AA_Assay.pdf, SB_OA_Assay.pdf |
Combined analysis:
| Analysis ID | AN000468 | AN000469 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Agilent 1290 Infinity | Thermo Dionex Ultimate 3000 |
| Column | Waters AccQ Tag (100 x 2mm,1.7um) | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole |
| MS instrument name | Agilent 6490 QQQ | Thermo Quantiva QQQ |
| Ion Mode | POSITIVE | POSITIVE |
| Units | uM | uM |
Chromatography:
| Chromatography ID: | CH000332 |
| Chromatography Summary: | Waters AccQ·Tag Amino Acid Assay |
| Methods Filename: | SB_AA_Assay.pdf |
| Instrument Name: | Agilent 1290 Infinity |
| Column Name: | Waters AccQ Tag (100 x 2mm,1.7um) |
| Column Temperature: | 55 |
| Flow Rate: | 0.7 mL/min |
| Solvent A: | AccQ·Tag Eluent A |
| Solvent B: | accQ·Tag Eluent B |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH000333 |
| Methods Filename: | SB_OA_Assay.pdf |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| Column Temperature: | 45 |
| Flow Rate: | 0.3 mL/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 100% acetonitrile; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
MS:
| MS ID: | MS000408 |
| Analysis ID: | AN000468 |
| Instrument Name: | Agilent 6490 QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| Ion Mode: | POSITIVE |
| Analysis Protocol File: | SB_AA_Assay.pdf |
| MS ID: | MS000409 |
| Analysis ID: | AN000469 |
| Instrument Name: | Thermo Quantiva QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| Ion Mode: | POSITIVE |
| Analysis Protocol File: | SB_OA_Assay.pdf |
