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MB Sample ID: SA071481

Local Sample ID:P7_2
Subject ID:SU001095
Subject Type:Mammal
Subject Species:Tursiops truncatus
Taxonomy ID:9739
Gender:Male and female

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Subject:

Subject ID:SU001095
Subject Type:Mammal
Subject Species:Tursiops truncatus
Taxonomy ID:9739
Gender:Male and female

Factors:

Local Sample IDMB Sample IDFactor Level IDLevel ValueFactor Name
P7_2SA071481FL011209SkinTissue

Collection:

Collection ID:CO001089
Collection Summary:Environmental samples.
Sample Type:Skin and Blubber
Collection Method:NA
Collection Tube Temp:4 C

Treatment:

Treatment ID:TR001109
Treatment Summary:None.

Sample Preparation:

Sampleprep ID:SP001102
Sampleprep Summary:A portion (about 20 mg) of each tissue extract was dissolved in 500 ml of phosphate buffer (pH = 7.0) and then 500 ml of deuterium oxide containing 0.05 % v/v trimethylsilane was added.

Analysis:

MB Sample ID:SA071481
Analysis ID:AN001722
Laboratory Name:Laboratorio Nacional de Nano y Biomateriales, CINVESTAV-Unidad Mérida
Analysis Type:NMR
Acquisition Date:June 13, 2018
Software Version:Vnmrj 2.3, Revision A
Operator Name:Dra. Gloria Ivonne Hernández Bolio
Detector Type:NA
Data Format:.fid
Num Factors:2
Num Metabolites:51
Units:Relative abundance

NMR:

NMR ID:NM000128
Analysis ID:AN001722
Instrument Name:Varian 600 MHz AR Premium Compact
Instrument Type:FT-NMR
NMR Experiment Type:1D 1H
Spectrometer Frequency:600 MHz
NMR Probe:OneProbe
NMR Solvent:D2O
NMR Tube Size:5 mm
Shimming Method:Gradient shimming
Pulse Sequence:PRESAT
Water Suppression:Yes, satmode
Pulse Width:5.90 (90°)
Power Level:63
Receiver Gain:20
Presaturation Power Level:20
Chemical Shift Ref Cpd:0 ppm (TSP)
Temperature:25
Number Of Scans:128
Acquisition Time:3
Relaxation Delay:2
Spectral Width:9615.4
Num Data Points Acquired:64000
Real Data Points:57692
Chemical Shift Ref Std:TSP
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