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MB Sample ID: SA001045


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Combined analysis:

Analysis ID AN000034 AN000035
Analysis type MS MS
Chromatography type Reversed phase Reversed phase
Chromatography system Agilent 1200 Agilent 1200
Column Waters Acquity HSS T3 reversed-phase Waters Acquity HSS T3 reversed-phase
MS Type ESI ESI
MS instrument type QTOF QTOF
MS instrument name Agilent 6530 QTOF Agilent 6530 QTOF
Ion Mode POSITIVE NEGATIVE
Units peak area peak area

Chromatography:

Chromatography ID:CH000017
Chromatography Summary:Positive ion detection
Methods Filename:EX00166-LCMS-method.pdf
Instrument Name:Agilent 1200
Column Name:Waters Acquity HSS T3 reversed-phase
Column Temperature:40C
Flow Gradient:0-0.5 min 1% B, 0.5-2 min 1-99% B, 2-6 min 99% B, 6-9 min 1% B.
Flow Rate:0.35 mL/min
Solvent A:100% water; 0.1% formic acid
Solvent B:100% methanol; 0.1% formic acid
Chromatography Type:Reversed phase
  
Chromatography ID:CH000018
Chromatography Summary:Negative ion detection
Methods Filename:EX00166-LCMS-method.pdf
Instrument Name:Agilent 1200
Column Name:Waters Acquity HSS T3 reversed-phase
Column Temperature:40C
Flow Gradient:0-0.5 min 1% B, 0.5-2 min 1-99% B, 2-6 min 99% B, 6-9 min 1% B.
Flow Rate:0.35 mL/min
Solvent A:100% water; 0.1% ammonium bicarbonate
Solvent B:100% methanol; 0.1% ammonium bicarbonate
Chromatography Type:Reversed phase
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