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MB Sample ID: SA034207
| Local Sample ID: | 228_CFS |
| Subject ID: | SU000640 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 53 ± 3.5 (23-69 yr) |
| Gender: | Male |
| Human Ethnicity: | White/non-Hispanic |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN000946 | AN000947 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | HILIC | HILIC |
| Chromatography system | Shimadzu 20AD | Shimadzu 20AD |
| Column | Shodex NH2P-40 2E (250× 2.0 mm) | Shodex NH2P-40 2E (250× 2.0 mm) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
| Ion Mode | NEGATIVE | POSITIVE |
| Units | AUC | AUC |
Chromatography:
| Chromatography ID: | CH000674 |
| Chromatography Summary: | hydrophilic interaction chromatography (HILIC) on shodex column |
| Instrument Name: | Shimadzu 20AD |
| Column Name: | Shodex NH2P-40 2E (250× 2.0 mm) |
| Column Pressure: | 900~2800 psi |
| Column Temperature: | 25 C |
| Flow Gradient: | 0-3.5 min: 95%B, 3.6-8 min: 85% B, 8.1-13 min: 75% B, 13.5–35 min: 0% B, 36–46 min: 95% B, 46.1 min: end. |
| Flow Rate: | 0.2 ml/min |
| Injection Temperature: | room temperature |
| Solvent A: | 95% water/5% acetonitrile; 20 mM ammonium carbonate; 38 mM ammonium hydroxide, pH 9.8 |
| Solvent B: | 100% acetonitrile |
| Analytical Time: | 46.1 min |
| Oven Temperature: | 25 C |
| Sample Loop Size: | 10 ul |
| Sample Syringe Size: | 100 ul |
| Chromatography Type: | HILIC |
