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MB Sample ID: SA042804
| Local Sample ID: | 17627 |
| Subject ID: | SU000807 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN001240 | AN001241 | AN001242 | AN001243 |
|---|---|---|---|---|
| Analysis type | MS | MS | MS | MS |
| Chromatography type | HILIC | HILIC | HILIC | HILIC |
| Chromatography system | Agilent 1290 Infinity | Agilent 1290 Infinity | Agilent 1290 Infinity | Agilent 1290 Infinity |
| Column | Waters XBridge Amide (100 x 4.6mm,3.5um) | Waters XBridge Amide (100 x 4.6mm,3.5um) | Phenomenex Luna NH2 (150 x 2.1mm,3um) | Phenomenex Luna NH2 (150 x 2.1mm,3um) |
| MS Type | ESI | ESI | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole | Triple quadrupole | Triple quadrupole |
| MS instrument name | Agilent 6490A QQQ | Agilent 6490A QQQ | Agilent 6490A QQQ | Agilent 6490A QQQ |
| Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
| Units | log transform with internal standard normalization | log transform with internal standard normalization | log transform with internal standard normalization | log transform with internal standard normalization |
Chromatography:
| Chromatography ID: | CH000867 |
| Chromatography Summary: | Flow rate was 0.3ml/min. Gradients were run starting from 85% buffer B (0.1% formic acid in acetonitrile) to 35% B from 0–3.5 minutes; 35% B to 2% B from 3.5–11.5 minutes; 2% B was held from 11.5–16.5 minutes; 2% B to 85% B from 16.5–17.5 minutes; 85% B was held for 7 minutes to re-equilibrate the column. |
| Instrument Name: | Agilent 1290 Infinity |
| Column Name: | Waters XBridge Amide (100 x 4.6mm,3.5um) |
| Flow Rate: | 0.3ml/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 100% acetonitrile; 0.1% formic acid |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH000868 |
| Chromatography Summary: | Flow rate was 0.3ml/min. Gradients were run starting from 85% buffer B (HPLC grade acetonitrile ) to 35% B from 0–3.5 minutes; 35% B to 2% B from 3.5–11.5 minutes; 2% B was held from 11.5–16.5 minutes; 2% B to 85% B from 16.5–17.5 minutes; 85% B was held for 7 minutes to re-equilibrate the column |
| Instrument Name: | Agilent 1290 Infinity |
| Column Name: | Phenomenex Luna NH2 (150 x 2.1mm,3um) |
| Flow Rate: | 0.3ml/min |
| Solvent A: | 100% water; 20 mM ammonium formate, pH 9 |
| Solvent B: | 100% acetonitrile |
| Chromatography Type: | HILIC |
