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MB Sample ID: SA051650

Local Sample ID:TP02
Subject ID:SU000924
Subject Type:Animal
Subject Species:Mus musculus
Taxonomy ID:10090
Species Group:Mammal

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Combined analysis:

Analysis ID AN001449
Analysis type MS
Chromatography type GC
Chromatography system Leco Pegasus 4D GC
Column Restek Rtx-5Sil (30m x 0.25mm,0.25um)
MS Type EI
MS instrument type GC x GC-TOF
MS instrument name Leco Pegasus 4D GCxGC TOF
Ion Mode POSITIVE
Units intensity

Chromatography:

Chromatography ID:CH001018
Chromatography Summary:GCMS analysis is based on the Oliver Fiehn method
Instrument Name:Leco Pegasus 4D GC
Column Name:Restek Rtx-5Sil (30m x 0.25mm,0.25um)
Column Pressure:14.05psi
Column Temperature:Initial Oven Temp 100⁰C, hold 60 sec. Ramp rate 20⁰C/min to 330⁰C, hold 5 min.
Flow Gradient:constant flow
Flow Rate:1 mL/min
Injection Temperature:250⁰C
Retention Index:FAME retention index markers C8-C30
Sample Injection:1.0 µL
Analytical Time:20 min
Oven Temperature:Initial Oven Temp100⁰C, hold 60 sec. Ramp rate 20⁰C/min to 330⁰C, hold 5 min.
Transferline Temperature:280⁰C
Chromatography Type:GC
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