Return to study ST000918 main page
MB Sample ID: SA054104
| Local Sample ID: | CP16 |
| Subject ID: | SU000956 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 35 - 65 |
| Weight Or Weight Range: | 61 - 75 |
| Gender: | Female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN001503 | AN001504 | AN001505 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | GC | Reversed phase | Reversed phase |
| Chromatography system | Agilent | Agilent 1200 | Agilent 1200 |
| Column | Zebron ZB-5MSi capillary GC | Phenomenex Kinetex C18 (150 x 2.1mm,2.6um) | Phenomenex Kinetex C18 (150 x 2.1mm,2.6um) |
| MS Type | EI | ESI | ESI |
| MS instrument type | Single quadrupole | QTOF | QTOF |
| MS instrument name | Agilent 5973 | Agilent 6530 QTOF | Agilent 6530 QTOF |
| Ion Mode | POSITIVE | POSITIVE | NEGATIVE |
| Units | peak area | peak area | peak area |
Chromatography:
| Chromatography ID: | CH001060 |
| Chromatography Summary: | Untargeted GC/MS method |
| Instrument Name: | Agilent |
| Column Name: | Zebron ZB-5MSi capillary GC |
| Column Temperature: | 0-1 min 60ªC 1-33 min to 320ªC |
| Flow Rate: | 1.0 mL/min |
| Sample Injection: | 2 uL |
| Chromatography Type: | GC |
| Chromatography ID: | CH001061 |
| Chromatography Summary: | Untargeted LC/MS method |
| Chromatography Comments: | HPLC system 1200 series coupled to Q-TOF 6520 |
| Instrument Name: | Agilent 1200 |
| Column Name: | Phenomenex Kinetex C18 (150 x 2.1mm,2.6um) |
| Column Pressure: | 300 bar |
| Column Temperature: | 40°C |
| Flow Gradient: | 25% B increased then to 95% B in 35 min, returned to initial conditions in 1 min and was kept constant for 9 min to ensure re-equilibration of the column |
| Flow Rate: | 0.3 mL/min |
| Sample Injection: | 10 uL |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 100% acetonitrile; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
