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MB Sample ID: SA059636
| Local Sample ID: | 360 |
| Subject ID: | SU001017 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | >30 |
| Gender: | Male and female |
| Human Inclusion Criteria: | Patients from the Hospital das Clínicas Outpatient Clinics ≥30 years-old and with at least two measurements of creatinine (with a minimum interval of 3 months) ≥1.6 mg/dL for men and ≥1.4 mg/dL for women were considered potential candidates. |
| Human Exclusion Criteria: | Patients attending oncology, psychiatry, urology, HIV/AIDS, viral hepatitis and glomerulonephritis services were excluded. The remaining candidates were then contacted by phone and invited to participate if no exclusion criteria were met (hospitalization or acute myocardial infarction in the last 6 months, autoimmune diseases, pregnancy, psychiatric diseases, ongoing chemo or immunosuppressive therapy, ongoing renal replacement therapy, glomerulonephritis, HIV/AIDS infection, hepatitis C and B, and any previous organ transplantation). |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN001602 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | Agilent 7890B |
| Column | DB5-MS + 10m Duraguard capillary (Agilent 122-5532G) |
| MS Type | EI |
| MS instrument type | Single quadrupole |
| MS instrument name | Agilent 5975C |
| Ion Mode | POSITIVE |
| Units | peak height |
Chromatography:
| Chromatography ID: | CH001124 |
| Instrument Name: | Agilent 7890B |
| Column Name: | DB5-MS + 10m Duraguard capillary (Agilent 122-5532G) |
| Column Temperature: | 60°C for 1 min, and then increased to 310°C at a rate of 10°C/min |
| Flow Rate: | 0.736ml/min |
| Injection Temperature: | 250C |
| Sample Injection: | 1uL |
| Analytical Time: | 37 minutes |
| Capillary Voltage: | 70eV |
| Oven Temperature: | 60°C for 1 min, and then increased to 310°C at a rate of 10°C/min |
| Weak Wash Solvent Name: | Methanol |
| Weak Wash Volume: | 3x 5uL |
| Strong Wash Solvent Name: | Isopropanol |
| Strong Wash Volume: | 3x 5uL |
| Sample Syringe Size: | 10uL |
| Chromatography Type: | GC |
