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MB Sample ID: SA069405

Local Sample ID:P2
Subject ID:SU001076
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Genotype Strain:NA
Age Or Age Range:NA
Gender:Male
Human Race:NA

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Combined analysis:

Analysis ID AN001698
Analysis type MS
Chromatography type GC
Chromatography system QEOrbitrap-GC-MS
Column TraceGOLD™ TG-5SILMS
MS Type EI
MS instrument type Orbitrap
MS instrument name Thermo Q Exactive Orbitrap
Ion Mode POSITIVE
Units Abundance

Chromatography:

Chromatography ID:CH001197
Chromatography Summary:A robotic arm TriPlus™ RSH autosampler (Thermo Scientific™, Bremen, Germany) injected 1µL of derivatized sample into a split/splitless (SSL) injector at 250 °C using a 1:100 split flow on TRACE™ 1310 gas chromatograph (Thermo Scientific™, Austin, TX). Helium carrier gas at a flow rate of 1 mL/min was used for separation on a Thermo Scientific™ TraceGOLD™ TG-5SILMS 30 m length × 0.25 mm i.d. × 0.25 µm film thickness column. The initial oven temperature was held at 70 °C for 4 min, followed by an initial gradient of 20 °C/min ramp rate. The final temperature was 320 °C and held for 8 min.
Instrument Name:QEOrbitrap-GC-MS
Column Name:TraceGOLD™ TG-5SILMS
Chromatography Type:GC
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