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MB Sample ID: SA076805
| Local Sample ID: | AG261114_43 |
| Subject ID: | SU001170 |
| Subject Type: | Chemical |
| Subject Species: | None |
| Subject Comments: | Primary standards of nucleotide triphosphates (ATP, GTP, UTP and CTP). |
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Combined analysis:
| Analysis ID | AN001822 |
|---|---|
| Analysis type | MS |
| Chromatography type | HILIC |
| Chromatography system | Waters Acquity |
| Column | Phenomenex Luna NH2 (100 x 2.0mm,3um) |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Waters Synapt G2 Si QTOF |
| Ion Mode | NEGATIVE |
| Units | Peak area |
Chromatography:
| Chromatography ID: | CH001291 |
| Chromatography Summary: | Untargeted HILIC Method |
| Instrument Name: | Waters Acquity |
| Column Name: | Phenomenex Luna NH2 (100 x 2.0mm,3um) |
| Column Temperature: | 20C |
| Flow Gradient: | 30% eluent A to 99% eluent A in 8 min, followed by isocratic elution at 99% eluent A until 14 min. A conditioning cycle of 6 min with the initial proportions of eluents A and B was performed prior to the next analysis. |
| Flow Rate: | 0.25 mL/min |
| Sample Injection: | 10 µL |
| Solvent A: | 100% water; 5 mM ammonium acetate, pH 9.9 |
| Solvent B: | 100% acetonitrile |
| Analytical Time: | 20 min |
| Chromatography Type: | HILIC |
