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MB Sample ID: SA080047
Local Sample ID: | C4 |
Subject ID: | SU001218 |
Subject Type: | Mammal |
Subject Species: | Mus musculus |
Taxonomy ID: | 10090 |
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Combined analysis:
Analysis ID | AN001903 |
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Analysis type | MS |
Chromatography type | GC |
Chromatography system | Thermo-finnegan DSQ |
Column | Restek 5% phenyl |
MS Type | EI |
MS instrument type | GC/MS |
MS instrument name | Thermo DSQ |
Ion Mode | UNSPECIFIED |
Units | AU |
Chromatography:
Chromatography ID: | CH001378 |
Chromatography Summary: | The samples destined for GC/MS analysis were re-dried under vacuum desiccation for a minimum of 24 hours prior to being derivatized under dried nitrogen using bistrimethyl-silyl-triflouroacetamide (BSTFA). The GC column was 5% phenyl and the temperature ramp is from 40° to 300° C in a 16 minute period. Samples were analyzed on a Thermo-Finnigan Trace DSQ fast-scanning single-quadrupole mass spectrometer using electron impact ionization. The instrument was tuned and calibrated for mass resolution and mass accuracy on a daily basis. The information output from the raw data files was automatically extracted as discussed below. |
Instrument Name: | Thermo-finnegan DSQ |
Column Name: | Restek 5% phenyl |
Chromatography Type: | GC |