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MB Sample ID: SA080920
Local Sample ID: | 0.1_48h_2 |
Subject ID: | SU001235 |
Subject Type: | Cultured cells |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Gender: | Not applicable |
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Combined analysis:
Analysis ID | AN001935 |
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Analysis type | MS |
Chromatography type | HILIC |
Chromatography system | Shimadzu LC-30A |
Column | Waters XBridge Amide (100 x 4.6mm,3.5um) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | ABI Sciex 5600 TripleTOF |
Ion Mode | NEGATIVE |
Units | normalized peak area |
Chromatography:
Chromatography ID: | CH001404 |
Chromatography Summary: | The mobile phase consisted of solvent A (5 mM ammonium acetate, pH=9, and 5% acetonitrile) and solvent B (acetonitrile). The gradient was set as follows: 0–3 min, 85% B; 3–6 min, 85–30% B; 6–15 min, 30–2% B; 15–18 min, 2% B; 18–19 min, 2–85% B; 19–26 min, 85% B. The flow rate was set at 0.4 mL/min. |
Instrument Name: | Shimadzu LC-30A |
Column Name: | Waters XBridge Amide (100 x 4.6mm,3.5um) |
Flow Gradient: | 0-3 min, 85% B; 3-6 min, 85-30% B; 6-15 min, 30-2% B; 15-18 min, 2% B; 18-19 min, 2-85% B; 19-26 min, 85% B. |
Flow Rate: | 0.4 mL/min |
Solvent A: | 5% acetonitrile/95% water; 5 mM ammonium acetate, pH 9 |
Solvent B: | 100% acetonitrile |
Chromatography Type: | HILIC |