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MB Sample ID: SA094336
| Local Sample ID: | 267 HZCD |
| Subject ID: | SU001377 |
| Subject Type: | Mammal |
| Subject Species: | Mus musculus |
| Taxonomy ID: | 10090 |
| Genotype Strain: | c57bl6 |
| Age Or Age Range: | 16 weeks |
| Gender: | Male |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002169 | AN002170 | AN002171 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | Reversed phase | Reversed phase | GC |
| Chromatography system | Agilent 1290 Infinity II | Agilent 1290 Infinity II | Agilent 7890B |
| Column | Poroshell 120 EC-C8 (100 x 2.1mm,2.5um) | Poroshell 120 EC-C8 (100 x 2.1mm,2.5um) | Agilent DB5-MS (30m x 0.25mm, 0.25um) |
| MS Type | ESI | ESI | EI |
| MS instrument type | QTOF | QTOF | GC QTOF |
| MS instrument name | Agilent 6545 | Agilent 6545 | Agilent 7890A |
| Ion Mode | POSITIVE | NEGATIVE | POSITIVE |
| Units | Area | Area | Area |
Chromatography:
| Chromatography ID: | CH001587 |
| Chromatography Summary: | LC-MS (+) |
| Instrument Name: | Agilent 1290 Infinity II |
| Column Name: | Poroshell 120 EC-C8 (100 x 2.1mm,2.5um) |
| Column Temperature: | 60 |
| Flow Gradient: | gradient started at 82% phase B, increasing to 90% B in 17 min. The gradient then increased to 100% B by minute 18 and was maintained for 2 minutes until 20 min. The starting condition was returned to by 21.5 min, followed by an 8.5 min reequilibration time, taking the total run time to 30 min |
| Flow Rate: | 0.5 mL/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 85% methanol/15% isopropanol; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH001588 |
| Chromatography Summary: | LC-MS (-) |
| Instrument Name: | Agilent 1290 Infinity II |
| Column Name: | Poroshell 120 EC-C8 (100 x 2.1mm,2.5um) |
| Column Temperature: | 60 |
| Flow Gradient: | gradient started at 82% phase B, increasing to 90% B in 17 min. The gradient then increased to 100% B by minute 18 and was maintained for 2 minutes until 20 min. The starting condition was returned to by 21.5 min, followed by an 8.5 min reequilibration time, taking the total run time to 30 min |
| Flow Rate: | 0.5 mL/min |
| Solvent A: | 100% water; 0.1% formic acid |
| Solvent B: | 85% methanol/15% isopropanol; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH001589 |
| Chromatography Summary: | GC-MS |
| Instrument Name: | Agilent 7890B |
| Column Name: | Agilent DB5-MS (30m x 0.25mm, 0.25um) |
| Chromatography Type: | GC |
