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MB Sample ID: SA185573
| Local Sample ID: | Pooled Human Plasma 2 |
| Subject ID: | SU002061 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Gender: | Pooled |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002856 |
|---|---|
| Analysis type | MS |
| Chromatography type | HILIC |
| Chromatography system | Agilent 1290 Infinity II |
| Column | Waters Acquity BEH Amide (100 x 2.1mm,1.7um) |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6545 |
| Ion Mode | POSITIVE |
| Units | Total Intensity Units |
Chromatography:
| Chromatography ID: | CH002383 |
| Chromatography Summary: | HILIC separations were performed on a Waters Acquity UPLC BEH amide column (2.1 x 100 mm 1.7 m) with a matching Vanguard precolumn. The flow rate was set to 0.3 mL/min and mobile phases consisted of (A) 95:5 acetonitrile/water with 0.125% v/v formic acid and 10 mM ammonium formate and (B) 95:5 water/acetonitrile with 0.125% v/v formic acid and 10 mM ammonium formate. Gradient specified in protocol file. |
| Methods Filename: | 2 mm amide pos MS2 70%H2O 120min_PC6.m |
| Instrument Name: | Agilent 1290 Infinity II |
| Column Name: | Waters Acquity BEH Amide (100 x 2.1mm,1.7um) |
| Column Pressure: | 300 bar |
| Column Temperature: | 55 |
| Flow Rate: | 0.3 mL/min |
| Sampling Cone: | 175 V |
| Solvent A: | 95% acetonitrile/5% water; 0.125% formic acid; 10 mM ammonium formate |
| Solvent B: | 5% acetonitrile/95% water; 0.125% formic acid; 10 mM ammonium formate |
| Analytical Time: | 120 min |
| Capillary Voltage: | 3500 V |
| Weak Wash Solvent Name: | 85:15 acetonitrile:water |
| Target Sample Temperature: | 4 |
| Sample Loop Size: | 20 uL |
| Chromatography Type: | HILIC |
