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MB Sample ID: SA208959

Local Sample ID:19 +DON 15N 3
Subject ID:SU002260
Subject Type:Other abiotic sample

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Combined analysis:

Analysis ID AN003562
Analysis type MS
Chromatography type HILIC
Chromatography system Ulitmate 3000
Column SeQuant ZIC-pHILIC (150 x 4.6mm,5um)
MS Type ESI
MS instrument type Triple quadrupole
MS instrument name Thermo Q Exactive Orbitrap
Ion Mode UNSPECIFIED
Units N/L

Chromatography:

Chromatography ID:CH002633
Chromatography Summary:SeQuant ZIC-pHILIC 5um polymer, 150x2.1mm - Part No. 15046000001 Buffer A: 10mM ammonium carbonate in water, LCMS Grade Buffer B: Acetonitrile, LCMS Grade Rear Wash: 10% methanol in water, LCMS Grade Wash Buffer: water, LCMS Grade Injection Volume: 2uL
Methods Filename:L12
Instrument Name:Ulitmate 3000
Column Name:SeQuant ZIC-pHILIC (150 x 4.6mm,5um)
Column Pressure:1800
Column Temperature:25
Flow Rate:0.100ml/min
Injection Temperature:4
Internal Standard:ISTD (500nM amino acid cocktail)
Solvent A:100% water; 10 mM ammonium carbonate
Solvent B:100% acetonitrile
Chromatography Type:HILIC
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