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MB Sample ID: SA155090
| Local Sample ID: | s44_2 |
| Subject ID: | SU001759 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 19-87 |
| Gender: | Male and female |
| Human Race: | Caucasian |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002746 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Shimadzu 20AD |
| Column | Waters Acquity BEH C18 (100 x 2mm,1.7um) |
| MS Type | ESI |
| MS instrument type | Other |
| MS instrument name | Shimadzu LCMS-IT-TOF |
| Ion Mode | POSITIVE |
| Units | area |
MS:
| MS ID: | MS002543 |
| Analysis ID: | AN002746 |
| Instrument Name: | Shimadzu LCMS-IT-TOF |
| Instrument Type: | Other |
| MS Type: | ESI |
| MS Comments: | The apparatus consisted of a two LC-20AD pumps (Shimadzu, Japan), an automatic sample injector, coupled on-line with an LCMS-IT-TOF (Shimadzu, Japan) mass spectrometer. The column effluent was analyzed by ESI-MS. MS detection was operated in positive ionisation mode with the following parameters: detector voltage, 1.53 kV; interface voltage, +4.5 kV; CDL (curve desolvation line) temperature, 200 ˚C; block heater temperature, 200 ˚C; nebulizing gas flow (He), 1.5 L/min; drying gas pressure, 100 kPa. Full scan MS data were acquired in the range of 80–850 m/z (ion accumulation time, 30 ms; event time, 300 ms; repeat = 3. |
| Ion Mode: | POSITIVE |
| Capillary Voltage: | +4.5 kV |
| Dry Gas Flow: | 100 kPa |
| Helium Flow: | 1.5 ml/min |
| Ion Source Temperature: | 200 ˚C |
| Ionization: | positive |
| Mass Accuracy: | 15 ppm |
| Source Temperature: | 200 ˚C |
| Cdl Temperature: | 200 ˚C |
