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MB Sample ID: SA210338
| Local Sample ID: | CNMI_32 |
| Subject ID: | SU002280 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN003591 | AN003592 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | CE | GC |
| Chromatography system | Agilent 7100 CE | 8890 |
| Column | silica capillary (100 cm; inner diameter,50um,Agilent Technologies) | Agilent DB5-MS (30m x 0.25mm, 0.25um) |
| MS Type | ESI | EI |
| MS instrument type | TOF | Single quadrupole |
| MS instrument name | Agilent CE-TOFMS | Agilent 5977B |
| Ion Mode | POSITIVE | UNSPECIFIED |
| Units | Peak Area | Corrected areas |
MS:
| MS ID: | MS003346 |
| Analysis ID: | AN003591 |
| Instrument Name: | Agilent CE-TOFMS |
| Instrument Type: | TOF |
| MS Type: | ESI |
| MS Comments: | Data were acquired in positive ionization polarity with a full scan range from 70 to 1000 m/z at a rate of 1.36 scan/s. The rest of MS conditions were: fragmentor set to 125 V, skimmer to 65 V, OCT RF Vpp to 750 V, drying gas temperature to 200 °C, flow rate to 10 L/min, nebulizer to 10 psig, and capillary voltage to 3500 V. The sheath liquid used for detection contained two reference masses (5 µL of purine with m/z 121.0509 and 5 µL of HP-0921 with m/z 922.0098) in MeOH/water (1/1; v/v) with 1 mM formic acid and the flow rate was set to 0.6 mL/min (split 1:100). The data acquisition was made using the Agilent MassHunter Workstation (Agilent Technologies). |
| Ion Mode: | POSITIVE |
| Analysis Protocol File: | Sample_Analysis.pdf |
| MS ID: | MS003347 |
| Analysis ID: | AN003592 |
| Instrument Name: | Agilent 5977B |
| Instrument Type: | Single quadrupole |
| MS Type: | EI |
| MS Comments: | The transfer line temperature was stablished at 280 °C and the electron ionization (EI) source was operated at 70 eV and the filament source temperature was set at 200 °C. Mass spectra were collected over a mass range of 50 - 600 m/z at a scan rate of 2.7 scans/s. Data were acquired using the Agilent MassHunter Workstation GC/MS Data Acquisition (version 10.0). |
| Ion Mode: | UNSPECIFIED |
| Analysis Protocol File: | Sample_Analysis.pdf |
