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MB Sample ID: SA052551
| Local Sample ID: | UR46 |
| Subject ID: | SU000928 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Select appropriate tab below to view additional metadata details:
Subject:
| Subject ID: | SU000928 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Species Group: | Human |
Factors:
| Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
|---|---|---|---|---|
| UR46 | SA052551 | FL009980 | Urine | SampleType |
Collection:
| Collection ID: | CO000922 |
| Collection Summary: | N/A |
| Sample Type: | Urine |
Treatment:
| Treatment ID: | TR000942 |
| Treatment Summary: | N/A |
Sample Preparation:
| Sampleprep ID: | SP000935 |
| Sampleprep Summary: | Mixing 540 μL of urine with 60 μL D2O potassium buffer + DSS |
| Extract Storage: | -80 C |
Analysis:
| MB Sample ID: | SA052551 |
| Analysis ID: | AN001453 |
| Analysis Type: | NMR |
| Acquisition Date: | 9/6/2016 | 9/6/2016 | 9/6/2016 | 9/6/2016 |
| Acquisition Parameters File: | urine-paper-160923/NOESYPR1D urine-paper-160923/PURGE_OPTIMIZED urine-paper-160923/NOESYGPPR1D urine-paper-160923/PURGE Raw File(s) (filename or directory) urine-paper-160923/NOESYPR1D urine-paper-160923/PURGE_OPTIMIZED urine-paper-160923/NOESYGPPR1D urine-paper-160923/PURGE |
| Software Version: | Topspin 3.5 pl 5 |
| Num Factors: | 1 |
NMR:
| NMR ID: | NM000109 |
| Analysis ID: | AN001453 |
| Instrument Name: | Bruker Avance III |
| Instrument Type: | FT-NMR |
| NMR Experiment Type: | 1D 1H |
| NMR Comments: | 4 spectra per sample: the first is the noesypr1d, then an optimized version of PURGE, then noesygppr1d, and finally the original PURGE (called zgpurge by Bruker) |
| Field Frequency Lock: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
| Spectrometer Frequency: | 600 MHz |
| NMR Probe: | TCI 600 H-C/N-D | TCI 600 H-C/N-D | TCI 600 H-C/N-D | TCI 600 H-C/N-D |
| NMR Solvent: | H2O+D2O (90/10) potassium buffer | H2O+D2O (90/10) potassium buffer | H2O+D2O (90/10) potassium buffer | H2O+D2O (90/10) potassium buffer |
| NMR Tube Size: | 5 mm | 5 mm | 5 mm | 5 mm |
| Shimming Method: | Topshim | Topshim | Topshim | Topshim |
| Pulse Sequence: | noesypr1d | zgpurge-gprefocus-4 | noesygppr1d | zgpurge |
| Water Suppression: | Presaturation | Presaturation | Presaturation | Presaturation |
| Pulse Width: | 19.94 μL | 19.94 μL | 19.94 μL | 19.94 μL |
| Power Level: | 5.5584 W | 5.5584 W | 5.5584 W | 5.5584 W |
| Receiver Gain: | 90.5 | 90.5 | 90.5 | 90.5 |
| Offset Frequency: | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz | 2824.58 Hz |
| Presaturation Power Level: | 0.000088411 W | 0.000088411 W | 0.000088411 W | 0.000088411 W |
| Chemical Shift Ref Cpd: | TSP | TSP | TSP | TSP |
| Temperature: | 300 K | 300 K | 300 K | 300 K |
| Number Of Scans: | 32 | 32 | 32 | 32 |
| Dummy Scans: | 4 | 4 | 4 | 4 |
| Acquisition Time: | 2.726 | 2.726 | 2.726 | 2.726 |
| Relaxation Delay: | 4 s | 4 s | 4 s | 4 s |
| Spectral Width: | 20.03 ppm | 20.03 ppm | 20.03 ppm | 20.03 ppm |
| Num Data Points Acquired: | 65536 | 65536 | 65536 | 65536 |
| Real Data Points: | 32768 | 32768 | 32768 | 32768 |
| Line Broadening: | 0.3 Hz | 0.3 Hz | 0.3 Hz | 0.3 Hz |
| Zero Filling: | 131072 | 131072 | 131072 | 131072 |
| Apodization: | Gaussian | Gaussian | Gaussian | Gaussian |
| Baseline Correction Method: | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 | Polynomial order 2 |
| Chemical Shift Ref Std: | DSS | DSS | DSS | DSS |
