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MB Sample ID: SA300852
| Local Sample ID: | 1281202_t |
| Subject ID: | SU002912 |
| Subject Type: | Cultured cells |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 63 - 73 |
| Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004561 |
|---|---|
| Analysis type | MS |
| Chromatography type | HILIC |
| Chromatography system | Shimadzu Prominence UFLC HPLC |
| Column | Waters XBridge Amide (100 x 4.6mm,3.5um) |
| MS Type | ESI |
| MS instrument type | QTRAP |
| MS instrument name | ABI Sciex 6500 QTrap |
| Ion Mode | UNSPECIFIED |
| Units | Q3 Peak Area (area under curve) |
Chromatography:
| Chromatography ID: | CH003427 |
| Methods Filename: | nprot_2012_024_v2.pdf |
| Instrument Name: | Shimadzu Prominence UFLC HPLC |
| Column Name: | Waters XBridge Amide (100 x 4.6mm,3.5um) |
| Column Temperature: | 475 |
| Flow Gradient: | Gradients were run with a Prominence UFLC HPLC (Shimadzu) starting from 85% buffer B (HPLC grade acetonitrile) to 42% B from 0-5 minutes; 42% B to 0% B from 5-16 minutes; 0% B was held from 16-24 minutes; 0% B to 85% B from 24-25 minutes; 85% B was held for 7 minutes to re-equilibrate the column. |
| Flow Rate: | 400uL/min |
| Solvent A: | 20 mM ammonium hydroxide/20 mM ammonium acetate (pH=9.0) in 95:5 water:acetonitrile |
| Solvent B: | HPLC grade acetonitrile |
| Chromatography Type: | HILIC |
