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MB Sample ID: SA317972
| Local Sample ID: | 12 |
| Subject ID: | SU003041 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Gender: | Male and female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004802 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Thermo Vanquish |
| Column | Waters ACQUITY UPLC BEH Amide (100 x 2.1mm,1.7um) |
| MS Type | ESI |
| MS instrument type | Orbitrap |
| MS instrument name | Thermo Q Exactive HF-X Orbitrap |
| Ion Mode | UNSPECIFIED |
| Units | % Total |
Chromatography:
| Chromatography ID: | CH003630 |
| Instrument Name: | Thermo Vanquish |
| Column Name: | Waters ACQUITY UPLC BEH Amide (100 x 2.1mm,1.7um) |
| Column Temperature: | 45 |
| Flow Gradient: | Run time was 25 min using a binary gradient starting at 20% B for 3 min, increasing to 45% B from 3 - 5.5 min, then to 65% B from 5.5 - 8 min, then to 85% B from 8 - 13 min, then to 100% B from 13 - 14 min. The gradient was held at 100% B from 14 - 20 min, then decreased to 20% B and held to 25 min. |
| Flow Rate: | 0.28 ml/min |
| Solvent A: | 60% acetonitrile/40% water; 10 mM ammonium formate; 0.1% formic acid |
| Solvent B: | 10% acetonitrile/90% isopropanol; 10 mM ammonium formate; 0.1% formic acid |
| Chromatography Type: | Reversed phase |
