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MB Sample ID: SA318529
| Local Sample ID: | 381 |
| Subject ID: | SU003050 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004817 | AN004818 | AN004819 | AN004820 | AN004821 | AN004822 |
|---|---|---|---|---|---|---|
| Analysis type | MS | MS | MS | MS | MS | MS |
| Chromatography type | Reversed phase | Reversed phase | HILIC | HILIC | None (Direct infusion) | None (Direct infusion) |
| Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Vanquish | Thermo Vanquish | Shimazdu LC-30AD | Shimazdu LC-30AD |
| Column | Agilent Zorbax SBaq (50 x 2.1mm x 1.7 um) | Agilent Zorbax SBaq (50 x 2.1mm x 1.7 um) | Merck SeQuant ZIC-HILIC (100 x 2.1mm,3.5um) | Merck SeQuant ZIC-HILIC (100 x 2.1mm,3.5um) | None | None |
| MS Type | ESI | ESI | ESI | ESI | ESI | ESI |
| MS instrument type | Orbitrap | Orbitrap | Orbitrap | Orbitrap | QTRAP | QTRAP |
| MS instrument name | Thermo Q Exactive Plus Orbitrap | Thermo Q Exactive Plus Orbitrap | Thermo Q Exactive HF hybrid Orbitrap | Thermo Q Exactive HF hybrid Orbitrap | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
| Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
| Units | Relative Abundance | Relative Abundance | Relative Abundance | Relative Abundance | Relative Abundance | Relative Abundance |
Chromatography:
| Chromatography ID: | CH003640 |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Agilent Zorbax SBaq (50 x 2.1mm x 1.7 um) |
| Column Temperature: | 60 |
| Flow Gradient: | N/A |
| Flow Rate: | 0.6 ml/min |
| Solvent A: | 0.06% acetic acid in water |
| Solvent B: | 0.06% acetic acid in methanol |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH003641 |
| Instrument Name: | Thermo Vanquish |
| Column Name: | Merck SeQuant ZIC-HILIC (100 x 2.1mm,3.5um) |
| Column Temperature: | 40 |
| Flow Gradient: | N/A |
| Flow Rate: | 0.5 ml/min |
| Solvent A: | 10 mM ammonium acetate in 50/50 acetonitrile/water |
| Solvent B: | 10 mM ammonium acetate in 95/5 acetonitrile/water |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH003642 |
| Instrument Name: | Shimazdu LC-30AD |
| Column Name: | None |
| Column Temperature: | 20 |
| Flow Gradient: | N/A |
| Flow Rate: | 0.15 ml/min |
| Solvent A: | 9:1 Methanol Toluene with 10 mM ammonium acetate |
| Solvent B: | N/A |
| Chromatography Type: | None (Direct infusion) |
