Summary of Study ST000101
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000089. The data can be accessed directly via it's Project DOI: 10.21228/M8988G This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
Study ID | ST000101 |
Study Title | NMR analysis of Synthetic Mixture Analysis |
Study Type | Synthetic |
Study Summary | Two groups of mixtures with 5 replicates each were each made using 20 synthetic metabolites. Some metabolites were at equal concentrations in both groups, and 10 metabolites differed between groups with half higher in group A, and half higher in group B. |
Institute | University of Florida |
Department | Department of Biochemistry and Molecular Biology and Southeastern Center for Integrated Metabolomics (SECIM) |
Laboratory | Arthur Edison |
Last Name | Edison |
First Name | Arthur |
Address | R3-226 Academic Research Building, Department of Biochemistry & Molecular Biology, PO Box 100245, Gainesville, FL 32610-0245 |
aedison@ufl.edu | |
Submit Date | 2014-09-15 |
Num Groups | 2 |
Total Subjects | 10 |
Raw Data Available | Yes |
Raw Data File Type(s) | fid |
Uploaded File Size | 11 M |
Analysis Type Detail | NMR |
Release Date | 2015-02-03 |
Release Version | 1 |
Select appropriate tab below to view additional metadata details:
NMR:
NMR ID: | NM000034 |
Analysis ID: | AN000167 |
Instrument Name: | Varian |
Instrument Type: | FT-NMR |
NMR Experiment Type: | 1D 13C |
Spectrometer Frequency: | 600 MHz |
NMR Probe: | 1.5 mm HTS cryoprobe |
NMR Solvent: | D2O |
NMR Tube Size: | 1.5 mm |
Shimming Method: | Manual |
Pulse Sequence: | 1D 13C |
Pulse Width: | 60 |
Receiver Gain: | 28 |
Temperature: | 22 degree Celsius |
Number Of Scans: | 8192 |
Dummy Scans: | 16 |
Acquisition Time: | 0.8s |
Relaxation Delay: | 0.1 |
Spectral Width: | 212 ppm |
Num Data Points Acquired: | 51282 |
Real Data Points: | 25641 |
Line Broadening: | 2 Hz |
Zero Filling: | 2x |
Apodization: | Exponential |
NMR ID: | NM000035 |
Analysis ID: | AN000168 |
Instrument Name: | Varian |
Instrument Type: | FT-NMR |
NMR Experiment Type: | 1D 1H |
Spectrometer Frequency: | 600 MHz |
NMR Probe: | 1.5 mm HTS cryoprobe |
NMR Solvent: | D2O |
NMR Tube Size: | 1.5 mm |
Shimming Method: | Manual |
Pulse Sequence: | 1D 1H |
Water Suppression: | Presaturation |
Pulse Width: | 45 |
Receiver Gain: | 28 |
Offset Frequency: | 4.77 |
Chemical Shift Ref Cpd: | TSP |
Temperature: | 22 degree Celsius |
Number Of Scans: | 64 |
Dummy Scans: | 16 |
Acquisition Time: | 2.0s |
Relaxation Delay: | 2s |
Spectral Width: | 12 ppm |
Num Data Points Acquired: | 32768 |
Real Data Points: | 16384 |
Zero Filling: | 2x |
Apodization: | Cosine squared |