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MB Sample ID: SA165096
| Local Sample ID: | LP25_pre_CSF_M |
| Subject ID: | SU001857 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 25(IQR 22-31) |
| Gender: | Male and female |
| Human Race: | European |
| Human Medications: | None |
| Human Prescription Otc: | None |
| Human Smoking Status: | None |
| Human Alcohol Drug Use: | None |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002890 | AN002891 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | HILIC | Reversed phase |
| Chromatography system | Shimadzu 20AD | Shimadzu 20AD |
| Column | Shodex NH2P-40 2E (250 x 2mm,4um) | Raptor Biphenyl (150 × 2.1 mm,2.7um) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
| Ion Mode | UNSPECIFIED | UNSPECIFIED |
| Units | peak area | peak area |
MS:
| MS ID: | MS002683 |
| Analysis ID: | AN002890 |
| Instrument Name: | ABI Sciex 5500 QTrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The MS/MS detection was performed using electrospray ionization (ESI) on both positive and negative modes. The MS/MS detection was performed using electrospray ionization (ESI) on both positive and negative modes. Advanced scheduled multiple reaction monitoring (MRM) with dynamic windowing and fast polarity switch were used. The ESI source conditions were set as follows: electrospray voltage of -4500 V for negative mode and 5500 V for positive mode, source temperature of 500 °C, curtain gas of 30, ion source gas 1, and gas 2 of 35 psi, respectively. |
| Ion Mode: | UNSPECIFIED |
| Collision Energy: | Compound-dependent |
| Collision Gas: | Medium |
| Ion Source Temperature: | 500 |
| Ion Spray Voltage: | -4500 V for negative and 5500 V for positive |
| Ionization: | ESI |
| Mass Accuracy: | 0.1 Da |
| Source Temperature: | 500 |
| MS ID: | MS002684 |
| Analysis ID: | AN002891 |
| Instrument Name: | ABI Sciex 5500 QTrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The MS/MS detection was performed using electrospray ionization (ESI) on both positive and negative modes. The MS/MS detection was performed using electrospray ionization (ESI) on both positive and negative modes. Advanced scheduled multiple reaction monitoring (MRM) with dynamic windowing and fast polarity switch were used. The ESI source conditions were set as follows: electrospray voltage of -4500 V for negative mode and 5500 V for positive mode, source temperature of 500 °C, curtain gas of 30, ion source gas 1, and gas 2 of 35 psi, respectively. |
| Ion Mode: | UNSPECIFIED |
| Collision Energy: | Compound-dependent |
| Collision Gas: | Medium |
| Ion Source Temperature: | 500 |
| Ion Spray Voltage: | -4500 V for negative and 5500 V for positive |
| Ionization: | ESI |
| Mass Accuracy: | 0.1 Da |
| Source Temperature: | 500 |
