Summary of study ST001037

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000694. The data can be accessed directly via it's Project DOI: 10.21228/M8ZT2M This work is supported by NIH grant, U2C- DK119886.

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Study IDST001037
Study TitleHigh Resolution GC-MS and FID Metabolomics of Human Serum
Study TypeHuman Serum Analysis
Study SummaryWe explored the possibility of performing quantitative metabolomics using a QEGC-MS using both FID and MS detectors as complementary techniques.
Institute
Wake Forest Baptist Medical Center
DepartmentCenter for Precision Medicine
LaboratoryMichael Olivier Laboratory
Last NameMisra
First NameBiswapriya
AddressMedical Center Boulevard NRC Building, G#43, Medical Center Boulevard, Winston Salem, NC, 27157, USA
Emailbbmisraccb@gmail.com
Phone3522156040
Submit Date2018-08-13
Total Subjects1
Num Males1
Study CommentsNA
PublicationsIn process
Raw Data AvailableYes
Raw Data File Type(s).raw
Analysis Type DetailGC-MS
Release Date2019-01-22
Release Version1
Biswapriya Misra Biswapriya Misra
https://dx.doi.org/10.21228/M8ZT2M
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

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Combined analysis:

Analysis ID AN001698
Analysis type MS
Chromatography type GC
Chromatography system QEOrbitrap-GC-MS
Column TraceGOLD™ TG-5SILMS
MS Type EI
MS instrument type Orbitrap
MS instrument name Thermo Q Exactive Orbitrap
Ion Mode POSITIVE
Units Abundance

Chromatography:

Chromatography ID:CH001197
Chromatography Summary:A robotic arm TriPlus™ RSH autosampler (Thermo Scientific™, Bremen, Germany) injected 1µL of derivatized sample into a split/splitless (SSL) injector at 250 °C using a 1:100 split flow on TRACE™ 1310 gas chromatograph (Thermo Scientific™, Austin, TX). Helium carrier gas at a flow rate of 1 mL/min was used for separation on a Thermo Scientific™ TraceGOLD™ TG-5SILMS 30 m length × 0.25 mm i.d. × 0.25 µm film thickness column. The initial oven temperature was held at 70 °C for 4 min, followed by an initial gradient of 20 °C/min ramp rate. The final temperature was 320 °C and held for 8 min.
Instrument Name:QEOrbitrap-GC-MS
Column Name:TraceGOLD™ TG-5SILMS
Chromatography Type:GC
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