Summary of Study ST001946

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001233. The data can be accessed directly via it's Project DOI: 10.21228/M8B99H This work is supported by NIH grant, U2C- DK119886.

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Study IDST001946
Study TitleBipolar disorder metabolomics analysis using FiehnLib and GMD for curation
Study TypeUntargeted GC analysis
Study SummaryIn this study we analyzed the blood serum from 14 controls and 14 BD patients using GC-MS under the conditions required for the use of FiehnLib library with GMD as secondary library for curation on a untargeted metabolomics approach
Institute
University of Campinas
DepartmentChemistry Institute, Department of Analytical Chemistry
LaboratoryLaboratory of Bioanalytics and Integrated Omics (LaBIOmics)
Last NameRibeiro
First NameHenrique
AddressRua Sérgio Buarque de Holanda,s/n
Emailhcarachoribeiro@gmail.com
Phone+55 19 3521 3018
Submit Date2021-10-11
Num Groups2
Total Subjects28
Num Males11
Num Females17
Raw Data AvailableYes
Raw Data File Type(s)cdf
Analysis Type DetailGC-MS
Release Date2021-11-04
Release Version1
Henrique Ribeiro Henrique Ribeiro
https://dx.doi.org/10.21228/M8B99H
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

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Combined analysis:

Analysis ID AN003168
Analysis type MS
Chromatography type GC
Chromatography system HP/Agilent 5890 Series II
Column HP5-MS (30m x 0.25mm x 0.25um) + Duragard precolumn (10m)
MS Type EI
MS instrument type Single quadrupole
MS instrument name HP 5970 Series Quadrupole Mass Selective Detector
Ion Mode UNSPECIFIED
Units Intensities after normalization by Internal standard and log2 transformed

Chromatography:

Chromatography ID:CH002341
Chromatography Summary:The following GC/MS conditions were used. An HP 5890 Series II oven was ramped by 10°C/min from 60°C (1 min initial time) to 325°C (10 min final time), resulting in a 37.5 min run time with cooling down to 60°C. 10 µL was injected into the Agilent split/splitless injector at 250°C in splitless mode. A 30 m long HP5-MS column with 10 m Duragard precolumn was used with 0.25 mm diameter and 0.25 µm film thickness. A constant flow rate of 1 mL/min helium was used as carrier gas. The quadrupole mass spectrometer was switched on after a 5.90 min solvent delay time, scanning from 50-600 u. The source temperature was set to 230°C and the quadrupole temperature was 150°C.
Instrument Name:HP/Agilent 5890 Series II
Column Name:HP5-MS (30m x 0.25mm x 0.25um) + Duragard precolumn (10m)
Chromatography Type:GC
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