Summary of Study ST001946
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001233. The data can be accessed directly via it's Project DOI: 10.21228/M8B99H This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST001946 |
| Study Title | Bipolar disorder metabolomics analysis using FiehnLib and GMD for curation |
| Study Type | Untargeted GC analysis |
| Study Summary | In this study we analyzed the blood serum from 14 controls and 14 BD patients using GC-MS under the conditions required for the use of FiehnLib library with GMD as secondary library for curation on a untargeted metabolomics approach |
| Institute | University of Campinas |
| Department | Chemistry Institute, Department of Analytical Chemistry |
| Laboratory | Laboratory of Bioanalytics and Integrated Omics (LaBIOmics) |
| Last Name | Ribeiro |
| First Name | Henrique |
| Address | Rua Sérgio Buarque de Holanda,s/n |
| hcarachoribeiro@gmail.com | |
| Phone | +55 19 3521 3018 |
| Submit Date | 2021-10-11 |
| Num Groups | 2 |
| Total Subjects | 28 |
| Num Males | 11 |
| Num Females | 17 |
| Raw Data Available | Yes |
| Raw Data File Type(s) | cdf |
| Analysis Type Detail | GC-MS |
| Release Date | 2021-11-04 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN003168 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | HP/Agilent 5890 Series II |
| Column | HP5-MS (30m x 0.25mm x 0.25um) + Duragard precolumn (10m) |
| MS Type | EI |
| MS instrument type | Single quadrupole |
| MS instrument name | HP 5970 Series Quadrupole Mass Selective Detector |
| Ion Mode | UNSPECIFIED |
| Units | Intensities after normalization by Internal standard and log2 transformed |
Chromatography:
| Chromatography ID: | CH002341 |
| Chromatography Summary: | The following GC/MS conditions were used. An HP 5890 Series II oven was ramped by 10°C/min from 60°C (1 min initial time) to 325°C (10 min final time), resulting in a 37.5 min run time with cooling down to 60°C. 10 µL was injected into the Agilent split/splitless injector at 250°C in splitless mode. A 30 m long HP5-MS column with 10 m Duragard precolumn was used with 0.25 mm diameter and 0.25 µm film thickness. A constant flow rate of 1 mL/min helium was used as carrier gas. The quadrupole mass spectrometer was switched on after a 5.90 min solvent delay time, scanning from 50-600 u. The source temperature was set to 230°C and the quadrupole temperature was 150°C. |
| Instrument Name: | HP/Agilent 5890 Series II |
| Column Name: | HP5-MS (30m x 0.25mm x 0.25um) + Duragard precolumn (10m) |
| Chromatography Type: | GC |
