Summary of Study ST001037
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000694. The data can be accessed directly via it's Project DOI: 10.21228/M8ZT2M This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST001037 |
| Study Title | High Resolution GC-MS and FID Metabolomics of Human Serum |
| Study Type | Human Serum Analysis |
| Study Summary | We explored the possibility of performing quantitative metabolomics using a QEGC-MS using both FID and MS detectors as complementary techniques. |
| Institute | Wake Forest Baptist Medical Center |
| Department | Center for Precision Medicine |
| Laboratory | Michael Olivier Laboratory |
| Last Name | Misra |
| First Name | Biswapriya |
| Address | Medical Center Boulevard NRC Building, G#43, Medical Center Boulevard, Winston Salem, NC, 27157, USA |
| bbmisraccb@gmail.com | |
| Phone | 3522156040 |
| Submit Date | 2018-08-13 |
| Total Subjects | 1 |
| Num Males | 1 |
| Study Comments | NA |
| Publications | In process |
| Raw Data Available | Yes |
| Raw Data File Type(s) | raw(Thermo) |
| Analysis Type Detail | GC-MS |
| Release Date | 2019-01-22 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN001698 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | QEOrbitrap-GC-MS |
| Column | TraceGOLD TG-5SILMS |
| MS Type | EI |
| MS instrument type | Orbitrap |
| MS instrument name | Thermo Q Exactive Orbitrap |
| Ion Mode | POSITIVE |
| Units | Abundance |
Chromatography:
| Chromatography ID: | CH001197 |
| Chromatography Summary: | A robotic arm TriPlus™ RSH autosampler (Thermo Scientific™, Bremen, Germany) injected 1µL of derivatized sample into a split/splitless (SSL) injector at 250 °C using a 1:100 split flow on TRACE™ 1310 gas chromatograph (Thermo Scientific™, Austin, TX). Helium carrier gas at a flow rate of 1 mL/min was used for separation on a Thermo Scientific™ TraceGOLD™ TG-5SILMS 30 m length × 0.25 mm i.d. × 0.25 µm film thickness column. The initial oven temperature was held at 70 °C for 4 min, followed by an initial gradient of 20 °C/min ramp rate. The final temperature was 320 °C and held for 8 min. |
| Instrument Name: | QEOrbitrap-GC-MS |
| Column Name: | TraceGOLD TG-5SILMS |
| Chromatography Type: | GC |
