Summary of Study ST002902
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001806. The data can be accessed directly via it's Project DOI: 10.21228/M88F0V This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
This study contains a large results data set and is not available in the mwTab file. It is only available for download via FTP as data file(s) here.
Study ID | ST002902 |
Study Title | Quantitative analysis of fatty acid compositions of retail cow’s milk and milk alternatives in Thailand using GC-MS |
Study Summary | All 36 brands of commercial milk samples available in retail stores in Thailand were collected in July 2019. They included 17 brands of whole cow’s milk, 6 brands of lactose-free cow’s milk, 9 brands of soymilk, and 4 brands of almond milk. Of all the cow’s milk samples, there were 6, 2, and 9 ultra-high temperature processing (UHT), sterilized, pasteurized milk samples, respectively. Quantification of fatty acids was performed using GC-MS. |
Institute | Mahidol University |
Department | Siriraj Metabolomics and Phenomics Center |
Laboratory | Siriraj Center of Research Excellence in Metabolomics and Systems Biology |
Last Name | Khoomrung |
First Name | Sakda |
Address | 2 Wanglang Road, Bangkok, Bangkok, 10700, Thailand |
sakda.kho@mahidol.edu | |
Phone | 024195511 |
Submit Date | 2023-09-25 |
Num Groups | 5 |
Total Subjects | 118 |
Publications | https://doi.org/10.1016/j.jfca.2020.103785 |
Raw Data Available | Yes |
Raw Data File Type(s) | mzML |
Analysis Type Detail | GC-MS |
Release Date | 2023-10-27 |
Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004761 |
---|---|
Analysis type | MS |
Chromatography type | GC |
Chromatography system | Leco Pegasus BT |
Column | Zebron ZB-FAME (30m × 0.25mm, 0.2um) |
MS Type | EI |
MS instrument type | GC-TOF |
MS instrument name | Agilent 7890B |
Ion Mode | POSITIVE |
Units | uMol |
Chromatography:
Chromatography ID: | CH003593 |
Chromatography Summary: | The upper phase containing FAMEs was taken for analysis using a GC coupled to a time of flight mass spectrometry (GC-TOFMS, Pegasus BT, Leco Corp., St.Joseph, MI) on a ZB-FAME (30 m ×0.25 mm ×0.2 μm, Zebron) in EI mode. One microliter of sample was injected with a split ratio of 60 to 1. Helium was used as a carrier gas. The total flow was 1 mL min−1. The GC oven temperature was programmed from 40 °C (2 min hold) to 150 °C at 20 °C min−1 (1 min hold), to 165 °C at 1 °C min−1 (1 min hold), to 180 °C at 2 °C min−1, to 200 °C at 5 °C min−1, and to 260 °C at 40 °C min−1 (8 min hold). The transfer line and ion source temperatures were kept at 240 °C and 220 °C, respectively. The TOFMS scanned from m/z 45–650 with a data acquisition rate of 20 spectra s−1. MS data was acquired and processed using ChromaTOF software (version 5.32, Leco Corp.). |
Instrument Name: | Leco Pegasus BT |
Column Name: | Zebron ZB-FAME (30m × 0.25mm, 0.2um) |
Column Temperature: | 40 |
Flow Gradient: | na |
Flow Rate: | 1 |
Solvent A: | na |
Solvent B: | na |
Chromatography Type: | GC |